A rapidly filled capillary mount for both dry powder and polycrystalline slurry samples | Zendy

Von Dreele R. B. | Zendy

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A rapidly filled capillary mount for both dry powder and polycrystalline slurry samples

Author(s) -

Von Dreele R. B.

Publication year - 2006

Publication title -

journal of applied crystallography

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.429

H-Index - 162

ISSN - 1600-5767

DOI - 10.1107/s002188980503284x

Subject(s) - slurry , crystallite , materials science , capillary action , tube (container) , powder diffraction , kapton , composite material , mineralogy , analytical chemistry (journal) , metallurgy , chromatography , crystallography , chemistry , polyimide , layer (electronics)

A method of rapid capillary sample loading of either dry powder or polycrystalline slurry has been developed. By embedding a Millipore filter in a Kapton capillary tube, one can then draw either loose dry powder or polycrystalline slurry into the tube and pack the solid against the filter, creating a dense column of powder suitable for a Debye–Scherrer powder diffraction experiment.

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