A cell for  in situ  dynamic X‐ray diffraction studies: application to the dehydration of zeolite SrX | Zendy

Palancher H. | Zendy; Pichon C. | Zendy; Rebours B. | Zendy; Hodeau J. L. | Zendy; Lynch J. | Zendy; Berar J. F. | Zendy; Prevot S. | Zendy; Conan G. | Zendy; Bouchard C. | Zendy

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A cell for in situ dynamic X‐ray diffraction studies: application to the dehydration of zeolite SrX

Author(s) -

Palancher H.,

Pichon C.,

Rebours B.,

Hodeau J. L.,

Lynch J.,

Berar J. F.,

Prevot S.,

Conan G.,

Bouchard C.

Publication year - 2005

Publication title -

journal of applied crystallography

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.429

H-Index - 162

ISSN - 1600-5767

DOI - 10.1107/s0021889805000294

Subject(s) - zeolite , in situ , synchrotron , dehydration , diffraction , materials science , homogeneity (statistics) , adsorption , x ray crystallography , characterization (materials science) , catalysis , chemical engineering , analytical chemistry (journal) , chemistry , nanotechnology , optics , chromatography , computer science , physics , organic chemistry , biochemistry , engineering , machine learning

A new compact cell for in situ synchrotron X‐ray diffraction studies of adsorption or catalysis reactions has been designed to enable high performance whilst minimizing difficulties in use. It includes a system for simple insertion and alignment of capillary samples and an original miniaturized furnace providing excellent temperature homogeneity along the sample (temperature gradient less than 1 K over a 6 mm zone at 530 K). The efficiency of this setup is illustrated by in situ characterization of a zeolite (SrX) at four hydration levels.

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