In situ  study of the formation of CdS nanoparticles by small‐angle X‐ray scattering | Zendy

Meneau Florian | Zendy; Cristol Sylvain | Zendy; Sankar Gopinathan | Zendy; Dolbnya Igor P | Zendy; Bras Wim | Zendy; Catlow C Richard A | Zendy; Thomas John M | Zendy; Greaves G Neville | Zendy

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In situ study of the formation of CdS nanoparticles by small‐angle X‐ray scattering

Author(s) -

Meneau Florian,

Cristol Sylvain,

Sankar Gopinathan,

Dolbnya Igor P,

Bras Wim,

Catlow C Richard A,

Thomas John M,

Greaves G Neville

Publication year - 2003

Publication title -

journal of applied crystallography

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.429

H-Index - 162

ISSN - 1600-5767

DOI - 10.1107/s0021889803000219

Subject(s) - small angle x ray scattering , nanoclusters , nanoparticle , scattering , cadmium sulfide , materials science , in situ , radius , sulfide , chemical engineering , small angle scattering , analytical chemistry (journal) , nanotechnology , chemistry , optics , physics , organic chemistry , metallurgy , computer security , engineering , computer science

Time‐resolved in situ small angle X‐ray scattering measurements were carried out to monitor the formation of nanoparticles of cadmium sulfide, from a solution containing the corresponding acetate and thioacetamide under solvothermal conditions. Analysis of the SAXS data shows that spherical cadmium sulfide particles of ca 105 Å in radius form within the first minutes of the reaction and then grow uniformly to form cylindrical nanoclusters over a period of a few hours, resulting in a highly monodispersed particles distribution.

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