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Diffraction thermometry and differential thermal analysis
Author(s) -
Kisi E. H.,
Riley D. P.
Publication year - 2002
Publication title -
journal of applied crystallography
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.429
H-Index - 162
ISSN - 1600-5767
DOI - 10.1107/s0021889802016497
Subject(s) - diffraction , differential thermal analysis , powder diffraction , materials science , phase transition , latent heat , differential (mechanical device) , precipitation , anomaly (physics) , phase (matter) , thermal , crystallography , thermodynamics , specific heat , analytical chemistry (journal) , chemistry , condensed matter physics , optics , physics , chromatography , meteorology , organic chemistry
A unit‐cell parameter anomaly observed during the precipitation and growth of Ti 3 SiC 2 from a Si‐substituted TiC phase is interpreted as the release of latent heat. The observations are used to propose a powder diffraction method for conducting differential thermal analysis as part of in situ phase transition studies.