Synthesis, characterization and gravimetric studies of novel triazole-based compound | Zendy

Ahmed A. AlAmiery | Zendy; Lina M. Shaker | Zendy; Abdul Amir H. Kadhum | Zendy; Mohd Sobri Takriff | Zendy

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Synthesis, characterization and gravimetric studies of novel triazole-based compound

Author(s) -

Ahmed A. AlAmiery,

Lina M. Shaker,

Abdul Amir H. Kadhum,

Mohd Sobri Takriff

Publication year - 2019

Publication title -

international journal of low-carbon technologies

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.458

H-Index - 26

eISSN - 1748-1325

pISSN - 1748-1317

DOI - 10.1093/ijlct/ctz067

Subject(s) - adsorption , corrosion , gravimetric analysis , fourier transform infrared spectroscopy , langmuir adsorption model , elemental analysis , scanning electron microscope , nuclear chemistry , thermogravimetric analysis , chemistry , infrared , characterization (materials science) , triazole , infrared spectroscopy , materials science , chemical engineering , inorganic chemistry , organic chemistry , nanotechnology , composite material , physics , optics , engineering

4-Amino-3-(2-bromo-5-methoxyphenyl)-1H-1,2,4-triazole-5(4H)-thione (ATH) was synthesized and characterized by nuclear magnetic resonance and Fourier-transform infrared as spectroscopical techniques and elemental analysis. ATH was studied for corrosion inhibition of mild steel in corrosive environment by means of weight loss technique, scanning electron microscopy and the adsorption isotherm. ATH demonstrates a superior inhibition efficiency against corrosion of mild steel. Adsorption data fit well to a Langmuir isotherm model.

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