Open AccessHydrothermal synthesis and characterization of Zinc Oxide nanoparticles of various shapes under different reaction conditions
Author(s) -
Sonima Mohan,
Mini Vellakkat,
Arun Aravind,
U Reka
Publication year - 2020
Publication title -
nano express
Language(s) - English
Resource type - Journals
ISSN - 2632-959X
DOI - 10.1088/2632-959x/abc813
Subject(s) - zinc , nanorod , hydrothermal circulation , nanoparticle , materials science , band gap , luminescence , grain size , chemical engineering , oxide , fourier transform infrared spectroscopy , absorption (acoustics) , hydrothermal synthesis , nanotechnology , inorganic chemistry , chemistry , metallurgy , composite material , optoelectronics , engineering
Zinc Oxide (ZnO) nanoparticles were synthesized by hydrothermal method under different conditions and studied various properties. FTIR studies proved the presence of ZnO bonding and purity of the samples. Grain size was found to be decreased with the increase of reaction temperature and increased with reaction time. TEM images show formation of nanorods under same reaction temperature, also nanoflowers and nanospheres for different temperatures. Intensity of luminescence peaks is found to be changed with variation in interplanar spacing. UV–vis spectra helped to identify the increased photon absorption in particles of bigger size. Change in bandgap value is also observed due to the difference in size of nanoparticles.