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Ultrathin mesoporous Ta 3 N 5  hollow nanospheres were synthesized via a facile and orchestrated template-free solution-based synthesis followed by thermal nitridation. A systematic investigation of structural evolution with annealing revealed a progressive crystallization with concurrent development of mesoporosity and modification of chemical composition with nitridation time. Subsequent performance of as-prepared photocatalysts were evaluated by the degradation of methylene blue under visible light irradiation ( λ  &gt; 400 nm). Ta 3 N 5  hollow nanospheres exhibited higher photocatalytic activity than Ta 3 N 5  nanorods or bulk Ta 3 N 5 , which can be attributed to their engineered structure as well as the oxygen and nitrogen content.

Template-free synthesis of Ta3N5 hollow nanospheres as a visible-light-driven photocatalyst

Template-free synthesis of Ta₃N₅ hollow nanospheres as a visible-light-driven photocatalyst