Nano-CaCO3 synthesis by jet-reactor from calcium carbide slag
Author(s) -
Shuaidong Mao,
Yan Liu,
Tingan Zhang,
Xiaolong Li
Publication year - 2020
Publication title -
materials research express
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.383
H-Index - 35
ISSN - 2053-1591
DOI - 10.1088/2053-1591/abc654
Subject(s) - scanning electron microscope , calcite , calcium hydroxide , materials science , saturation (graph theory) , volumetric flow rate , nano , particle size , calcium carbonate , chemical engineering , analytical chemistry (journal) , calcium carbide , carbide , mineralogy , nuclear chemistry , metallurgy , chemistry , composite material , chromatography , thermodynamics , combinatorics , engineering , mathematics , physics
Nano-CaCO 3 was producted by using carbide slag in the self-designed jet-reactor. The effect of different operating parameter such as CO 2 flow rate and concentration, liquid flow rate and concentration of Ca(OH) 2 on the CaCO 3 particle size and morphology has been investigated in this paper. The obtained calcite particle were characterized using x-ray diffraction (XRD) and scanning electron microscopy (SEM). The results showed that the calcite about 50–200 nm was obtained under the reaction conditions of the saturation of calcium hydroxide as 1, the flow rate as 1.5 l min −1 , the CO 2 flow rate as 50 ml min −1 , the concentration as 100%, and the SDS amount 2%.
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