Open AccessCharacterisation of super duplex stainless steel by optimisation of EBSD parameters
Author(s) -
Mona Haukali,
Ida Westermann,
Morten Karlsen,
Yingda Yu,
René de Kloe,
Jarle Hjelen
Publication year - 2020
Publication title -
iop conference series: materials science and engineering
Language(s) - English
Resource type - Journals
ISSN - 1757-8981
DOI - 10.1088/1757-899x/891/1/012013
Subject(s) - electron backscatter diffraction , intermetallic , materials science , microstructure , search engine indexing , metallurgy , alloy , austenite , artificial intelligence , computer science
Electron backscatter diffraction (EBSD) was used to characterise the microstructure of a super duplex stainless steel (SDSS) alloy Zeron 100 and the intermetallic phases sigma and chi in this material. The material was analysed in three conditions; as-received, heat-treated at 900 °C for 8 min and heat-treated at 750 °C for 4 h. Heat treatments were performed to introduce the intermetallic phases in the steel. It is difficult to get reliable indexing of the sigma and chi phases due to noisy and overlapping patterns. To get the best results, the Hough transformation parameters were optimised and an averaging technique was used. The optimisation was done by removing some of the reflectors in the sigma- and chi-phases in the original TSL material files used for pattern indexing. By changing Hough parameters, considerable improvements in the indexing of the patterns were observed along with the increase of average confidence index (CI) value for both intermetallic phases. The applied SEM, Zeiss Ultra 55 FESEM was equipped with a NORDIF UF-1100 EBSD detector to acquire and stream patterns to HD. Indexing and data processing were performed by TSL/OIM 7.3. In the present study, at the most four different phases are present in the SDSS.