
Synthesis and Adsorption Properties of Insoluble Starch Xanthate (ISX)
Author(s) -
Haihua Li,
Lihui Zhang,
Yuhua Gao,
Zhenfa Liu
Publication year - 2020
Publication title -
iop conference series. materials science and engineering
Language(s) - English
Resource type - Journals
eISSN - 1757-899X
pISSN - 1757-8981
DOI - 10.1088/1757-899x/735/1/012026
Subject(s) - xanthate , chemistry , adsorption , starch , fourier transform infrared spectroscopy , nuclear chemistry , sulfur , copper , catalysis , inorganic chemistry , organic chemistry , chemical engineering , engineering
Starch xanthate was synthesized from corn starch and CS 2 under alkaline condition. The effects of catalyst dosage, CS 2 dosage and reaction temperature on sulfur content and copper ion removal rate were studied by single factor experiments, and the structure of the product was characterized by FTIR, SEM and XRD. The results showed that the optimum synthetic condition of ISX was NaOH dosage 16 mL, CS 2 dosage 2.5 mL, reaction temperature 35 °C and reaction time 2 h. The sulfur content of ISX synthesized under this condition was 7.54%, the removal rate of copper ion was 90.5%, and the adsorption capacity of ISX was 90.0 mg/g.