Open AccessInfluence of varied process parameters on the microstructure, densification and microhardness of spark plasma sintered Ti-6Al-4V/h-BN binary composite
Author(s) -
John Olorunfemi Abe,
A. P. I. Popoola,
Olawale Popoola
Publication year - 2019
Publication title -
iop conference series. materials science and engineering
Language(s) - English
Resource type - Journals
eISSN - 1757-899X
pISSN - 1757-8981
DOI - 10.1088/1757-899x/689/1/012005
Subject(s) - materials science , microstructure , indentation hardness , spark plasma sintering , composite number , dwell time , composite material , ceramic , sintering , metallurgy , medicine , clinical psychology
The influence of varied process parameters involving three levels of temperature, pressure, heating rate and dwell time on the microstructure, densification and microhardness of spark plasma sintered Ti-6Al-4V/ h -BN binary composite was studied. Taguchi design method was adopted to randomize the SPS process parameter levels. The microstructure was analyzed by optical microscopy, densification was determined based on the principle of Archimedes and Vickers microhardness tester was used to evaluate the microhardness of the sintered composite. The consolidation of Ti-6Al-4V powder and nanoparticles of 3 wt.% of h -BN via SPS produced nearly full theoretical densification of 99.77% and the sintered composite gave a microhardness value of 710.37 HV which is more than 200% that of the monolithic alloy. The best combination of relative densification and microhardness were obtained at the sintering parameters of 1000 °C of temperature, 40 MPa of pressure, 100 °C/min heating rate and 15 min of dwell time. Generally, it was found that improved microstructure, densification and microhardness were influenced by the high temperature of sintering and low rate of heating that gave room for adequate diffusional mass transport resulting in solid bonding between the particles of the matrix and the ceramic reinforcement.