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Preparation and characterization of Pd93Cu7/Al2o3 composite membrane for hydrogen permeation
Author(s) -
Ratna Sari,
Sri Mulyati,
Ratni Dewi,
Lukman Hakim
Publication year - 2019
Publication title -
iop conference series materials science and engineering
Language(s) - English
Resource type - Journals
eISSN - 1757-899X
pISSN - 1757-8981
DOI - 10.1088/1757-899x/536/1/012114
Subject(s) - permeation , scanning electron microscope , membrane , selectivity , analytical chemistry (journal) , hydrogen , materials science , ceramic , nuclear chemistry , chemistry , chromatography , catalysis , metallurgy , composite material , organic chemistry , biochemistry
In this work, an electroless plating technique was used to prepare Pd-Cu coated ceramic alumina membranes tube. The composition, surface morphology and cross-section of the Pd 97 Cu 7 /Al 2 O 3 membrane is investigated by energy-dispersive spectrometry (EDS), and scanning electron microscopy (SEM). Hydrogen permeation and selectivity across a membrane is measured using pressure difference (1.05-1.5) at a temperature range (573-773 K). The reported membrane obtained a high flux of 3.4 mol H / ms at a temperature of 723 K, while the selectivity is above 75 for H 2 / N 2 .

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