
The influence of sample preparation techniques on results of extraction of heavy metals from soil
Author(s) -
Marina Burachevskaya,
Tatiana Minkina,
Saglara Mandzhieva,
V. S. Cicuashvili,
Elena Fedorenko,
Pavel Pogonyshev,
G. Coskun,
Rıdvan Kızılkaya
Publication year - 2020
Publication title -
iop conference series. earth and environmental science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.179
H-Index - 26
eISSN - 1755-1307
pISSN - 1755-1315
DOI - 10.1088/1755-1315/579/1/012004
Subject(s) - sieve (category theory) , fractionation , contamination , extraction (chemistry) , sample preparation , reagent , environmental chemistry , sample (material) , soil test , grinding , chemistry , heavy metals , soil contamination , soil water , environmental science , chromatography , metallurgy , soil science , materials science , mathematics , ecology , combinatorics , biology
A study of the composition of mobile compounds of heavy metals (HM) in the area of aerosol contamination by a heat supply company showed an increase in the number of these compounds near the source of contamination. In the group of loosely bound compounds, the largest part is represented by specifically sorbed compounds. Sample preparation (the degree of sample grinding) had a noticeable effect on the extractability of Zn, Cu, and Pb from the soil. During the sifting of a soil sample through a 0.25 mm sieve, the extraction of mobile forms of HM increases significantly (by 7–16 %). Thus, with an increase in the specific surface of soil particles, the extracting ability of the reagents increases. It is necessary to take into account the sample preparation used in each fractionation method to evaluate the results and compare them.