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Carbon Aerogels Preparation With Kaolin addition
Author(s) -
Yuelong Xu,
Bin Ren,
Zhenfa Liu
Publication year - 2020
Publication title -
iop conference series. earth and environmental science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.179
H-Index - 26
eISSN - 1755-1307
pISSN - 1755-1315
DOI - 10.1088/1755-1315/565/1/012039
Subject(s) - carbonization , resorcinol , scanning electron microscope , materials science , raman spectroscopy , carbon fibers , chemical engineering , specific surface area , texture (cosmology) , polymerization , sodium carbonate , porosity , catalysis , analytical chemistry (journal) , chemistry , polymer , sodium , chromatography , organic chemistry , composite material , computer science , optics , metallurgy , physics , image (mathematics) , artificial intelligence , composite number , engineering
Wet gels (WGs) have been obtained from the polymerization of phloroglucinol (P), resorcinol (R) and formaldehyde (F) using sodium carbonate (C) as catalyst with kaolin (KL) addition. Carbon aerogels (CAs) have been gotten through the carbonization of WGs. The porous texture properties of as - prepared samples are investigated using the surface-area analyzer. The crystal structure of CAs are studied by X-ray diffraction (XRD) and the degree of graphitization are obtained through a Raman spectrometer. Meanwhile scanning electron microscopy (SEM) are executed to observe the morphology of different samples. When the addition of 5 wt%, the samples exhibit the high specific surface area (SSA), up to 855m 2 g –1 , with a concentrated pore size disdribution (PSD) of 30 nm.