Open AccessOptical and Morphology Properties of the Magnetite ( Fe3O4) Nanoparticles Prepared by Green Method
Author(s) -
Rusul Mohammed Abdallah,
Raad M. S. Al-Haddad
Publication year - 2021
Publication title -
journal of physics. conference series
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.21
H-Index - 85
eISSN - 1742-6596
pISSN - 1742-6588
DOI - 10.1088/1742-6596/1829/1/012022
Subject(s) - magnetite , absorbance , nanoparticle , materials science , spectroscopy , dispersity , analytical chemistry (journal) , superparamagnetism , particle size , chemical engineering , nanotechnology , nuclear chemistry , chemistry , magnetization , chromatography , magnetic field , polymer chemistry , metallurgy , physics , quantum mechanics , engineering
Magnetite nanoparticles have been synthesized by a green method. For this process, ferricchloride hexahydrate, ferrouschloride tetrahydrate (2/1 molar ratio) solution was mixed with different amounts of carob leaves extract and NaOH solution was added to get pH(2, 5,8 and 11) heated for 30 min at (30,60,80 and 100) °C . In this report, a description was introduced for the synthesis of Fe 3 0 4 nanoparticles (NPs) in order to obtain the optimum (pH8 ,temperature and amount of extract) that have small particle size MNPs. The magnetite nanoparticles were characterized by UV-Vis absorption spectroscopy, through Field emission scanning electron microscopy (FESEM) and Atomic Force Microscope (AFM). In UV-Vis spectroscopy, the absorbance of surface plasmon resonance (SPR) of magnetite nanoparticles synthesized with different parameters, were observed a single visible peak located in the range of (290-519) nm and it was related to spherical monodisperse, peak shifts to shorter wavelength (blue shift) with change parameter. FESEM images confirm the Fe 3 0 4 NPs synthesized with different parameters were spherical shaped and lower than 50 nanoscale. AFM images of magnetite nanoparticles with different parameter. It is observed that each nucleus magnetite Nanoparticles is spherical in geometry