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Characterization of Fe, Ni, Pb Standard Solution using One-point Calibration Methods
Author(s) -
Eka Mardika Handayani,
Isna Komalasari,
Oman Zuas,
Christine Elishian,
Rosi Ketrin
Publication year - 2019
Publication title -
journal of physics. conference series
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.21
H-Index - 85
eISSN - 1742-6596
pISSN - 1742-6588
DOI - 10.1088/1742-6596/1338/1/012008
Subject(s) - calibration , traceability , certified reference materials , standard uncertainty , primary standard , standard solution , analytical chemistry (journal) , standard addition , characterization (materials science) , relative standard deviation , materials science , measurement uncertainty , chemistry , detection limit , mathematics , chromatography , nanotechnology , statistics
Calibration of measurement systems using well-prepared calibration materials is an important means of making traceability in chemical measurements. Traceability is established through the use of measurement standards (such as certified reference materials) that are appropriate for each parameter. Pure substance certified reference materials such as elemental standard solutions are the most commonly used for calibration, called external calibrations using one, two or multiple standards. In this study, one-point calibration method has been applied for characterizing of Fe, Ni and Pb standard solutions. The results show that the concentration of the Fe, Ni and Pb standard solutions with their relative uncertainties were found to be 997.81 ± 6.34 mg/kg, 997.61 ± 8.10 mg/kg, 1004.29 ± 8.62 mg/kg, respectively.

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