Single-scan ultra-selective 1D total correlation spectroscopy | Zendy

P. Király | Zendy; Mathias Nilsson | Zendy; Gareth A. Morris | Zendy; Ralph W. Adams | Zendy

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Single-scan ultra-selective 1D total correlation spectroscopy

Author(s) -

P. Király,

Mathias Nilsson,

Gareth A. Morris,

Ralph W. Adams

Publication year - 2021

Publication title -

chemical communications

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.837

H-Index - 333

eISSN - 1364-548X

pISSN - 1359-7345

DOI - 10.1039/d0cc08033k

Subject(s) - two dimensional nuclear magnetic resonance spectroscopy , spectroscopy , nuclear magnetic resonance spectroscopy , correlation , spectral line , nuclear magnetic resonance , materials science , chemistry , analytical chemistry (journal) , physics , organic chemistry , mathematics , geometry , quantum mechanics , astronomy

Selective 1D TOCSY is a powerful tool in the assignment of NMR spectra of organic molecules. Here an order of magnitude improvement in selectivity, allowing overlapping multiplets to be excited separately, is achieved in a single scan using the very recent GEMSTONE method. The new experiment is illustrated using an antibiotic and a mixture of diastereomers.

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