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A three-dimensional supramolecular framework containing both left- and right-handed helixes, {[Zn(TTPA)Cl 2 ]·1.63H 2 O}  n  ( 1 ), has been converted to a novel octanuclear cluster containing a metal-organic framework, [Zn 8 (ptptp) 6 Cl 2 ](ClO 4 ) 2 ·4CH 3 OH·2H 2 O ( 1b ), induced by ligand rearrangement during a solvothermal process. The luminescent properties of 1b indicate that the material can act as a selective probe toward Pb 2+ and Cr 2 O 7  2- .

acs omega

Ligand-Rearrangement-Induced Transformation from a 3D Supramolecular Network to a Discrete Octanuclear Cluster: A Good Detector for Pb2+ and Cr2O72–