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Stacking layered metal hydroxide films parallel to a substrate is challenging. Here, we demonstrate a simple and rapid electrodeposition method for stacking magnesium hydroxide layered films. Room-temperature cathodic electrolysis (40 mA cm -2 ) in a Mg(NO 3 ) 2 aqueous solution induces the deposition of ⟨001⟩-oriented Mg(OH)  x  layered films stacked parallel to the substrate at the deposition rate of ∼2 μm min -1 . The obtained Mg(OH)  x  layered films undergo an overall oriented transformation by heat treatment to form ⟨111⟩-oriented nanoporous MgO films.

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Electrochemical Growth of Mg(OH)<sub><i>x</i></sub> Layered Films Stacked Parallel to the Substrates and Their Thermal Conversion to (111)-Oriented Nanoporous MgO Films

Electrochemical Growth of Mg(OH)x Layered Films Stacked Parallel to the Substrates and Their Thermal Conversion to (111)-Oriented Nanoporous MgO Films

Electrochemical Growth of Mg(OH)_x Layered Films Stacked Parallel to the Substrates and Their Thermal Conversion to (111)-Oriented Nanoporous MgO Films