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A cyclic tetrapeptide L comprising two l-proline and two 3-amino-5-(pyridin-4-yl)benzoic acid subunits assembles into a dimetallic metallamacrocycle Pd   2   L   2  and a trimetallic coordination cage Pd   3   L   6  in the presence of suitable palladium(II) precursors. Pd   2   L   2  recognizes organic anions in aqueous media, forming a particularly stable complex with sodium 2,6-naphthalenedisulfonate, in which two dianionic guest molecules reside in the cavity surrounded by the cyclopeptide ligands.

Palladium(II)-Mediated Assembly of a M2L2 Macrocycle and M3L6 Cage from a Cyclopeptide-Derived Ligand

Palladium(II)-Mediated Assembly of a M₂L₂ Macrocycle and M₃L₆ Cage from a Cyclopeptide-Derived Ligand