A simple method for the preparation of 3,5-dinitrimino-1,2,4-triazole and its salts | Zendy

A. M. Astakhov | Zendy; Денис В. Антишин | Zendy; Виталий А. Ревенко | Zendy; A. D. Vasiliev | Zendy; É. S. Buka | Zendy

AI Assistant Blog Pricing

Home ZAIA Blog

Open Access

A simple method for the preparation of 3,5-dinitrimino-1,2,4-triazole and its salts

Author(s) -

A. M. Astakhov,

Денис В. Антишин,

Виталий А. Ревенко,

A. D. Vasiliev,

É. S. Buka

Publication year - 2017

Publication title -

chemistry of heterocyclic compounds

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.295

H-Index - 34

eISSN - 1573-8353

pISSN - 0009-3122

DOI - 10.1007/s10593-017-2116-7

Subject(s) - chemistry , semicarbazide , alkali metal , 1,2,4 triazole , hydrazine (antidepressant) , salt (chemistry) , metal , alkaline earth metal , organic chemistry , inorganic chemistry , chromatography

Текст статьи не публикуется в открытом доступе в соответствии с политикой журнала.The reaction of 2-methyl-1-nitrоisothiourea with hydrazine in the presence of alkali metal bicarbonates (carbonates) resulted in the formation of 3,5-dinitrimino-1,2,4-triazole salts. The same salts were also formed by a reaction of 2-methyl-1-nitrоisothiourea with alkali metal salts of 4-nitrоsemicarbazide. This represents the first synthesis and characterization of the high-energy 3,5-dinitrimino-1,2,4-triazole, which can be readily isolated by treatment of its disodium salt with HCl

The content you want is available to Zendy users.

Already have an account? Click here to sign in.

Having issues? You can contact us here

Accelerating Research