An X-ray microprobe facility using synchrotron radiation
Author(s) -
B.M. Gordon,
K.W. Jones,
A.L. Hanson,
Joel G. Pounds,
Mark L. Rivers,
P. Spanne,
S. R. Sutton
Publication year - 1990
Publication title -
biological trace element research
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.649
H-Index - 80
eISSN - 1559-0720
pISSN - 0163-4984
DOI - 10.1007/bf02992666
Subject(s) - microprobe , synchrotron radiation , optics , synchrotron , micrometer , x ray fluorescence , materials science , analytical chemistry (journal) , radiochemistry , fluorescence , physics , chemistry , mineralogy , chromatography
An X-ray microprobe for trace elemental analysis at micrometer spatial resolutions, using synchrotron radiation (SR), is under development. The facility consists of two beamlines, one including a 1:1 focusing mirror and the other an 8:1 ellipsoidal mirror. At present, "white light" is used for excitation of the characteristic X-ray fluorescence lines. Sensitivities in thin biological samples are in the range of 2-20 fg in 100 microns2 areas in 5 min irradiation times. Scanning techniques, as well as microtomography and chemical speciation, are discussed. Application to a specific biomedical study is included.
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