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Bisoxathiolane sulfides from a dioxoene fatty acid
Author(s) -
Mustafa J.,
Saeed M. T.,
Osman S. M.
Publication year - 1991
Publication title -
journal of the american oil chemists' society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.512
H-Index - 117
eISSN - 1558-9331
pISSN - 0003-021X
DOI - 10.1007/bf02657683
Subject(s) - acetic acid , elemental analysis , reagent , chemistry , mass spectrometry , fatty acid , infrared spectroscopy , spectroscopy , infrared , nuclear magnetic resonance spectroscopy , nuclear chemistry , organic chemistry , chromatography , physics , quantum mechanics , optics
A quantitative preparation of bisoxathiolane from 9,12‐dioxo‐ trans ‐10‐octadecenoic acid is discussed. The reagents used are β‐mercaptoethanol and BF 3− etherate in acetic acid. The structure of the product was established with the help of elemental analysis, infrared, nuclear magnetic resonance and mass spectroscopy data.