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Integrated system for microreactor gas chromatography
Author(s) -
Bitner E. D.,
Davison V. L.,
Dutton H. J.
Publication year - 1969
Publication title -
journal of the american oil chemists' society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.512
H-Index - 117
eISSN - 1558-9331
pISSN - 0003-021X
DOI - 10.1007/bf02541221
Subject(s) - microreactor , solenoid valve , ozone , solenoid , generator (circuit theory) , process engineering , chemistry , saponification , gas chromatography , reagent , chromatography , organic chemistry , engineering , electrical engineering , catalysis , physics , thermodynamics , power (physics)
A compact unit has been constructed to control and to supply a microreactor apparatus. Features are an ozone generator, gas flow rotameters, solenoid‐operated six‐way gas valve and a combination temperature‐and‐ozone meter. The meter monitors and, by means of a built‐in relay, controls reaction temperature. It also affords a visual indication of ozone concentration during reactions. Basic electronic circuits and common laboratory items simplify the unit's construction. Some possible microreactions to which this integrated system may be applied are ozonizationpyrolysis, esterification, transesterification, saponification, reduction and halogenation.