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Convenient preparation of methyl 10‐(1,3,2‐Oxazaphospholidin‐2‐one)undecanoate and methyl 10‐(1,3,2‐diazaphospholidin‐2‐one)undecanoate
Author(s) -
Saeed M. T.,
Mustafa J.,
Rauf A.,
Osman S. M.
Publication year - 1994
Publication title -
journal of the american oil chemists' society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.512
H-Index - 117
eISSN - 1558-9331
pISSN - 0003-021X
DOI - 10.1007/bf02540598
Subject(s) - ethylenediamine , chemistry , phosphorus , medicinal chemistry , nuclear chemistry , organic chemistry
Synthesis and spectral studies of methyl 10‐(1,3,2‐oxazaphospholidin‐2‐one)undecanoate and methyl 10‐(1,3,2‐diazaphospholidin‐2‐one)undecanoate are reported. These fatty products were obtained in excellent yields when methyl 10‐hydroxyundecanoate was reacted with phosphorus oxychloride, and the resultant intermediate was treated with aminoethanol and ethylenediamine in two different reactions.