Synthesis and X‐ray Crystal Structures of Homotrimetallic Zinc Bisureate Complexes | Zendy

Bayram Melike | Zendy; Wölper Christoph | Zendy; Schulz Stephan | Zendy

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Synthesis and X‐ray Crystal Structures of Homotrimetallic Zinc Bisureate Complexes

Author(s) -

Bayram Melike,

Wölper Christoph,

Schulz Stephan

Publication year - 2018

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.201700350

Subject(s) - zinc , heteronuclear molecule , chemistry , crystallography , crystal structure , x ray crystallography , elemental analysis , urea , nuclear magnetic resonance spectroscopy , single crystal , x ray , spectroscopy , alkane , stereochemistry , inorganic chemistry , diffraction , organic chemistry , catalysis , physics , quantum mechanics , optics

Alkane elimination reactions of the tethered bis(urea) proligand 1,4‐( t BuNHCONH) 2 ‐C 4 H 8 ( 1 ) with Zn R 2 ( R = Me, Et, n Pr) yielded trimetallic zinc complexes [ R Zn‐1,4‐( t BuNHCON) 2 ‐C 4 H 8 ] 2 Zn [ R = Me ( 2 ), Et ( 3 ), and n Pr ( 4 )]. 2 – 4 were characterized by heteronuclear NMR ( 1 H, 13 C) and IR spectroscopy, elemental analysis, and single‐crystal X‐ray diffraction.

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