Synthesis and Characterization of an Azobenzene‐Functionalized Ethene‐Bridged PMO | Zendy

Gräfenstein Lydia | Zendy; Venkatachalam Sabarinathan | Zendy; van Wüllen Leo | Zendy; Bensch Wolfgang | Zendy

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Synthesis and Characterization of an Azobenzene‐Functionalized Ethene‐Bridged PMO

Author(s) -

Gräfenstein Lydia,

Venkatachalam Sabarinathan,

van Wüllen Leo,

Bensch Wolfgang

Publication year - 2014

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.201300489

Subject(s) - azobenzene , materials science , spectroscopy , elemental analysis , sorption , characterization (materials science) , infrared spectroscopy , nuclear magnetic resonance spectroscopy , solid state , polymer chemistry , photochemistry , molecule , chemistry , nanotechnology , organic chemistry , adsorption , physics , quantum mechanics

The azobenzene‐functionalized ethene‐bridged periodic mesoporous organosilica (PMO) was synthesized in a three step process. After synthesizing the pure PMO the azobenzene switch was post synthetically grafted at the ethene bridge. The successful synthesis was verified by N 2 sorption measurements, IR spectroscopy, elemental analysis, and solid state MAS‐NMR spectroscopy. The switching process of the azobenzene was proven by UV/Vis measurements.

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