Synthesis, Crystal Growth and Structure of Substituted Mayenite | Zendy

Ebbinghaus Stefan | Zendy; Krause Holger | Zendy; Lerch Martin | Zendy; Janek Jürgen | Zendy

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Synthesis, Crystal Growth and Structure of Substituted Mayenite

Author(s) -

Ebbinghaus Stefan,

Krause Holger,

Lerch Martin,

Janek Jürgen

Publication year - 2010

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.201009108

Subject(s) - materials science , crystallography , crystal structure , crystal growth , chemical engineering , chemistry , engineering

International audienceBy simultaneous deposition of zinc and lithium onto a cooled sapphire substrate, LiZn₁₃ was obtained for the first time. It crystallizes in the NaZn₁₃ structure type (Fm3¯c, a = 1234.92(6) pm, Rp = 5.4%, Rwp = 6.9%, structure analysis with the Rietveld-method). Single-phase LiZn₁₃ forms from a hexagonal Li_0.07Zn_0.93 alloy, deposited at -196 °C, during heating up to room temperature. Above room temperature LiZn₁₃ decomposes

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