Synthesis and Crystal Structures of  t ‐Butyl‐Pyridine Adducts of Zn R  2  ( R  = Me,  i ‐Pr,  t ‐Bu, Cp*) | Zendy

Schulz Stephan | Zendy; Schäper Raphaela | Zendy; Krech Daniel | Zendy; Schuchmann Daniella | Zendy; Bläser Dieter | Zendy; Boese Roland | Zendy

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Synthesis and Crystal Structures of t ‐Butyl‐Pyridine Adducts of Zn R 2 ( R = Me, i ‐Pr, t ‐Bu, Cp*)

Author(s) -

Schulz Stephan,

Schäper Raphaela,

Krech Daniel,

Schuchmann Daniella,

Bläser Dieter,

Boese Roland

Publication year - 2011

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.201000264

Subject(s) - adduct , pyridine , chemistry , lewis acids and bases , crystallography , base (topology) , nuclear magnetic resonance spectroscopy , infrared spectroscopy , spectroscopy , medicinal chemistry , stereochemistry , catalysis , organic chemistry , physics , mathematical analysis , mathematics , quantum mechanics

Lewis acid‐base adducts of the general type R 2 Zn(4‐ t BuPy) x ( R = Me 1 , i Pr 2 , t Bu 3 , Cp* 4 ; x = 1, 2) were obtained in high yields from reactions of Zn R 2 with the Lewis base 4‐ t Bu‐Pyridine. Compounds 1 – 4 were characterized by multinuclear NMR ( 1 H, 13 C) and IR spectroscopy and elemental analyses, 1 and 4 also by X‐ray diffraction at single crystals.

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