Electron Microscopy Investigations on Highly Beam and Moisture Sensitive Samples – the System Li/Ba/Ca | Zendy

Kienle Lorenz | Zendy; Smetana Volodymyr | Zendy; Duppel Viola | Zendy; Simon Arndt | Zendy

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Electron Microscopy Investigations on Highly Beam and Moisture Sensitive Samples – the System Li/Ba/Ca

Author(s) -

Kienle Lorenz,

Smetana Volodymyr,

Duppel Viola,

Simon Arndt

Publication year - 2010

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.200900335

Subject(s) - crystallite , transmission electron microscopy , crystallography , materials science , electron microscope , crystal structure , analytical chemistry (journal) , electron beam processing , mineralogy , irradiation , chemistry , nanotechnology , optics , physics , chromatography , nuclear physics

The system Li/Ba/Ca was investigated by transmission electron microscopy (TEM). Three different phases could be identified and characterized. The crystal structure of the previously known compound Li 33.3 Ba 13.1 Ca 3 was confirmed, however, variable calcium contents were observed in distinct crystallites. The same holds for phases with BaLi 4 ‐ and Ba 19 Li 44 ‐type structure, respectively. Structural transformations under irradiation occurred which were different for the crystallites of the Li 33.3 Ba 13.1 Ca 3 ‐ and Ba 19 Li 44 ‐types.

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