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Elektrochemische Synthese von Ag 5 Pb 2 O 6
Author(s) -
Oberndorfer C. P. M.,
Jansen M.
Publication year - 2007
Publication title -
zeitschrift für anorganische und allgemeine chemie
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.354
H-Index - 66
eISSN - 1521-3749
pISSN - 0044-2313
DOI - 10.1002/zaac.200600284
Subject(s) - crystallite , electrochemistry , materials science , anode , rietveld refinement , ionic conductivity , aqueous solution , analytical chemistry (journal) , nuclear chemistry , crystallography , inorganic chemistry , mineralogy , chemistry , metallurgy , crystal structure , electrode , organic chemistry , electrolyte
Electrochemical Synthesis of Ag 5 Pb 2 O 6 Ag 5 Pb 2 O 6 was prepared by anodic oxidation of silver in a PbO 2 suspension in an aqueous KOH solution. Phase purity was checked by a Rietveld‐fit of the X‐ray powder pattern, thermal and chemical analysis. The compound exhibits ionic conductivity. It' anisotropy leads to an orientation of the crystallites on the silver anode.