Chains of OH − ‐centered [Pb 2+ ] 3  Triangles in the Crystal Structure of Pb 3 (OH) 2 (NH 2 SO 3 ) 4 | Zendy

Wickleder Mathias S. | Zendy

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Chains of OH − ‐centered [Pb 2+ ] 3 Triangles in the Crystal Structure of Pb 3 (OH) 2 (NH 2 SO 3 ) 4

Author(s) -

Wickleder Mathias S.

Publication year - 2005

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.200500176

Subject(s) - orthorhombic crystal system , crystallography , cationic polymerization , crystal structure , aqueous solution , chemistry , crystal (programming language) , materials science , polymer chemistry , computer science , programming language

Colourless single crystals of Pb 3 (OH) 2 (NH 2 SO 3 ) 4 were obtained hydrothermally by the reaction of PbO with NH 2 SO 3 H in aqueous solution. In the crystal structure (orthorhombic, Z = 8, Pnma , a = 2018.5(2), b = 2184.5(2), c = 722.19(6) pm, R 1 = 0.0757 (all data), OH − centred [Pb 2+ ] 3 triangles are connected to infinite cationic chains $^{1}_{\infty}\rm [(OH)Pb_{3/2}]^{2+}$ that are coordinated by the NH 2 SO 3 − ligands.

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