Pb 2 (OH) 2 [ p ‐O 2 C‐C 6 H 4 ‐CO 2 ]: Synthese und Kristallstruktur | Zendy

Schuy Andrea | Zendy; Ruschewitz Uwe | Zendy

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Pb 2 (OH) 2 [ p ‐O 2 C‐C 6 H 4 ‐CO 2 ]: Synthese und Kristallstruktur

Author(s) -

Schuy Andrea,

Ruschewitz Uwe

Publication year - 2005

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.200400485

Subject(s) - monoclinic crystal system , terephthalic acid , crystal structure , crystallography , hydrothermal synthesis , hydrothermal reaction , hydrothermal circulation , chemistry , stereochemistry , organic chemistry , seismology , polyester , geology

Pb 2 (OH) 2 [ p ‐O 2 C‐C 6 H 4 ‐CO 2 ]: Synthesis and Crystal Structure Single crystals of Pb 2 (OH) 2 [ p ‐O 2 C‐C 6 H 4 ‐CO 2 ] ( 1 ) were obtained by hydrothermal reaction of terephthalic acid and PbCO 3 at 180 °C (10 days). 1 crystallizes in the monoclinic space group P2 1 /c with Z = 2 (a = 1115.6(2) pm, b = 380.10(4) pm, c = 1141.3(2) pm, β = 93.39(1)°, V = 0.4831(1) nm 3 ). The crystal structure is characterized by ladder‐type Pb(OH) 3/3 double chains, which are connected to a three‐dimensional framework by terephthalate dianions.

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