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Präparation und Charakterisierung von PbBr 2 ·C 4 H 10 O 3 (Diethylenglykol)
Author(s) -
Oldag Thorsten,
Keller HansLothar
Publication year - 2004
Publication title -
zeitschrift für anorganische und allgemeine chemie
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.354
H-Index - 66
eISSN - 1521-3749
pISSN - 0044-2313
DOI - 10.1002/zaac.200300268
Subject(s) - monoclinic crystal system , crystallography , chemistry , x ray crystallography , group (periodic table) , crystal structure , single crystal , diffraction , physics , optics , organic chemistry
Structural Chemistry of PbBr 2 ·C 4 H 10 O 3 (Diethyleneglycol) Crystals of PbBr 2 ·C 4 H 10 O 3 have been synthesized and structurally characterized by single‐crystal X‐ray diffraction. PbBr 2 ·C 4 H 10 O 3 crystallizes monoclinic in space group P2 1 /n (No. 14) with a = 9.370(1)Å, b = 10.045(1)Å, c = 21.090(1)Å, β = 98.98(1)° and Z = 8. The compound contains compact Pb—Br groups, which build colums parallel to [0 1 0] direction by Hydrogen Bonding.