Zur Synthese von Na 3 FeO 3 , einem ternären Oxoferrat(III) mit Kettenstruktur | Zendy

Sobotka Bettina M. | Zendy; Möller Angela | Zendy

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Zur Synthese von Na 3 FeO 3 , einem ternären Oxoferrat(III) mit Kettenstruktur

Author(s) -

Sobotka Bettina M.,

Möller Angela

Publication year - 2003

Publication title -

zeitschrift für anorganische und allgemeine chemie

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.354

H-Index - 66

eISSN - 1521-3749

pISSN - 0044-2313

DOI - 10.1002/zaac.200300206

Subject(s) - crystallography , ternary operation , crystal structure , chemistry , metal , single crystal , materials science , organic chemistry , computer science , programming language

Synthesis of Na 3 FeO 3 , a Ternary Oxoferrate(III) with a Chain Structure Na 3 FeO 3 has been obtained from a redox reaction between CdO and iron metal in the presence of Na 2 O and Na 2 CO 3 at 650 °C as amber colored transparent single crystals. The crystal structure determination (IPDS data: P2 1 /n, a = 579.9(1) pm, b = 1265.9(2) pm, c = 582.8(1) pm, β = 116.02(2)°, Z = 4, R all = 0.0576) reveals the presence of ∞ 1 [FeO 2 O 2/2 ] zig‐zag‐chains.

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