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Die Kristallstruktur von tert ‐Butylimidomethylindan, [CH 3 InNC(CH 3 ) 3 ] 4
Author(s) -
Schmid K.,
Kühner S.,
Hausen H.D.,
Weidlein J.
Publication year - 1997
Publication title -
zeitschrift für anorganische und allgemeine chemie
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.354
H-Index - 66
eISSN - 1521-3749
pISSN - 0044-2313
DOI - 10.1002/zaac.19976231004
Subject(s) - crystal structure , chemistry , yield (engineering) , molar ratio , lithium (medication) , crystallography , amine gas treating , x ray crystallography , materials science , physics , diffraction , catalysis , organic chemistry , medicine , metallurgy , endocrinology , optics
The X‐Ray Structure Determination of tert ‐Butylimido Methylindane, [CH 3 InNC(CH 3 ) 3 ] 4 The reaction of MeInCl 2 with LiN(H) t Bu in a 1 : 2 molar ratio forms [MeInN t Bu] 4 in high yield, lithium chloride, and the free amine H 2 N t Bu. The crystal structure of the imidomethylindane with a cubic In 4 N 4 skeleton has been determined.