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Preparation and constitution of the Crystalline Silicic Acid Trimethylsilyl Ester [(CH 3 ) 3 Si] 6 Si 6 O 15
Author(s) -
Hoebbel D.,
Engelhardt G.,
Samoson A.,
Újszászy K.,
Smolin Yu. I.
Publication year - 1987
Publication title -
zeitschrift für anorganische und allgemeine chemie
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.354
H-Index - 66
eISSN - 1521-3749
pISSN - 0044-2313
DOI - 10.1002/zaac.19875520927
Subject(s) - trimethylsilyl , silicic acid , silicic , chemistry , silicate , mass spectrometry , ring (chemistry) , organic chemistry , geology , chromatography , geochemistry , volcano
A new crystalline compound has been synthesized by trimethylsilylation of tetraethylammonium silicate which was identified by means of gas chromatography, mass spectrometry, 29 Si NMR and X‐ray analysis to be a eage‐like double three‐ring silicic acid trimethylsilyl ester containing six inequivalent SiO 4 tetrahedra and trimethylsilyl groups.