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Facile Synthesis of Silver Hydroxyapatite (AgHAP) Reinforced Nanocomposites of Poly (styrene)‐Poly (methyl methacrylate) and Study of Their Mechanical and Blood‐Compatible Behavior
Author(s) -
Choubey Rashmi,
Chouhan Raje,
Bajpai Jaya,
Bajpai Anil Kumar
Publication year - 2019
Publication title -
chemistryselect
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.437
H-Index - 34
ISSN - 2365-6549
DOI - 10.1002/slct.201902351
Subject(s) - nanocomposite , materials science , methyl methacrylate , fourier transform infrared spectroscopy , zeta potential , nanoparticle , chemical engineering , poly(methyl methacrylate) , methacrylate , polymer , polystyrene , polymer chemistry , composite material , nuclear chemistry , copolymer , nanotechnology , chemistry , engineering
The present work focused on the synthesis of native silver hydroxyapatite (AgHAP) nanoparticles and their reinforcement into the host matrix of binary polymer blend of polystyrene (PS) and poly (methyl methacrylate) (PMMA). The structural and morphological studies of prepared nanoparticles and AgHAP reinforced PS‐PMMA nanocomposites were performed by various characterization techniques like Fourier transform infrared (FT‐IR) and Raman spectroscopy, X‐ray diffraction, atomic force microscopy (AFM), and Field emission scanning electron microscopy (FESEM). The particle size analysis and zeta potential measurements were used to confirm nanosize of the AgHAP nanoparticles and their surface charges. The mechanical properties of AgHAP/PS/PMMA nanocomposites, such as microhardness and compressive strength, were also determined. The blood compatibility tests were performed to investigate biocompatible nature of the nanocomposites. The antibacterial property of the nanocomposites was also studied against S. aureus and E. coli species and the cytotoxic nature of the nanocomposites was conducted following 3‐(4,5‐Dimethylthiazol‐2‐Yl)‐2,5‐Diphenyltetrazolium Bromide (MTT) assay test.