Eschenmoser‐Coupling Reaction Furnishes Diazenyl‐1,2,4‐triazole‐5(4 H )‐thione Derivatives | Zendy

Hassan Alaa A. | Zendy; Mohamed Nasr K. | Zendy; Aly Ashraf A. | Zendy; Tawfeek Hendawy N. | Zendy; Bräse Stefan | Zendy; Nieger Martin | Zendy

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Eschenmoser‐Coupling Reaction Furnishes Diazenyl‐1,2,4‐triazole‐5(4 H )‐thione Derivatives

Author(s) -

Hassan Alaa A.,

Mohamed Nasr K.,

Aly Ashraf A.,

Tawfeek Hendawy N.,

Bräse Stefan,

Nieger Martin

Publication year - 2019

Publication title -

chemistryselect

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.437

H-Index - 34

ISSN - 2365-6549

DOI - 10.1002/slct.201802870

Subject(s) - chemistry , nucleophile , 1,2,4 triazole , coupling reaction , coupling (piping) , reaction conditions , medicinal chemistry , crystal structure , combinatorial chemistry , organic chemistry , catalysis , materials science , metallurgy

Diazenyl 1,2,4‐triazol‐5(4 H )‐thione derivatives were synthesized in good yields via Eschenmoser‐coupling reaction and nucleophilic attack between 1,4‐disubstituted thiosemicarbazides and 2,3,5,6‐tetrachloro‐1,4‐benzoquinone ( p ‐CHL). The structure of the synthesized compounds was confirmed by IR, NMR and mass spectral data as well as single crystal X‐ray analysis.

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