New 1,1’‐Ferrocene Bis(sulfonyl) Reagents | Zendy

Chanawanno Kullapa | Zendy; Holstrom Cole | Zendy; Nemykin Victor N. | Zendy; Herrick Richard S. | Zendy; Ziegler Christopher J. | Zendy

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New 1,1’‐Ferrocene Bis(sulfonyl) Reagents

Author(s) -

Chanawanno Kullapa,

Holstrom Cole,

Nemykin Victor N.,

Herrick Richard S.,

Ziegler Christopher J.

Publication year - 2016

Publication title -

chemistryselect

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.437

H-Index - 34

ISSN - 2365-6549

DOI - 10.1002/slct.201601748

Subject(s) - sulfonyl , ferrocene , reagent , chemistry , organic chemistry , electrochemistry , alkyl , electrode

Several new 1,1’‐bis(sulfonyl)ferrocenes designed for the synthesis of sulfonamide linked biological conjugates have been prepared. 1,1’‐Bis(sulfonylbromide)ferrocene can be produced from the corresponding sulfonylchloride via a bis(sulfonylhydrazide) intermediate. Bis(sulfonyl‐ N ‐hydroxybenzotriazole)ferrocene can also be synthesized from the sulfonyl chloride, and reaction of glycine methyl ester with the sulfonyl chloride affords a [3]ferrocenophane complex. All new compounds have been structurally characterized by X‐ray crystallography.

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