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Inspection of morphology and elemental imaging of single nanoparticles by high‐resolution SEM/EDX in transmission mode
Author(s) -
Hodoroaba VasileDan,
Rades Steffi,
Unger Wolfgang E. S.
Publication year - 2014
Publication title -
surface and interface analysis
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.52
H-Index - 90
eISSN - 1096-9918
pISSN - 0142-2421
DOI - 10.1002/sia.5426
Subject(s) - nanoparticle , nanomaterials , transmission (telecommunications) , morphology (biology) , characterization (materials science) , materials science , high resolution , mode (computer interface) , nanotechnology , resolution (logic) , frame (networking) , spectroscopy , optics , computer science , physics , telecommunications , artificial intelligence , geology , paleontology , remote sensing , quantum mechanics , operating system
In the frame of the European project NanoValid , potential candidates of reference nanomaterials are manufactured and systematically characterized in particular with respect to their morphology (shape, size and size distribution). In this study, by exploiting the transmission operation mode in a high‐resolution SEM, known as transmission SEM, the potential of this methodical approach is demonstrated by means of representative examples of nanoparticles. The method enables quick and accurate morphological inspection and systematic characterization. Energy dispersive X‐ray spectroscopy imaging of single nanoparticles by using the transmission mode is demonstrated as feasible, too. Copyright © 2014 John Wiley & Sons, Ltd.

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