z-logo
open-access-imgOpen Access
Thermomechanical Formation and Recovery of Nanoindents in a Shape Memory Polymer Studied Using a Heated Tip
Author(s) -
Yang Fuzheng,
Wornyo Edem,
Gall Ken,
King William P.
Publication year - 2007
Publication title -
scanning
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.359
H-Index - 47
eISSN - 1932-8745
pISSN - 0161-0457
DOI - 10.1002/sca.20074
Subject(s) - polymer , materials science , shape memory polymer , glass transition , annealing (glass) , atomic force microscopy , acrylate , composite material , nanometre , indentation , atmospheric temperature range , polymer chemistry , nanotechnology , copolymer , thermodynamics , physics
This paper investigates the thermomechanical formation and recovery of nanometer‐scale indents in a shape memory polymer (SMP), studied using a heated atomic force microscope (AFM) tip and hot‐stage atomic force microscopy. The material tested is a tert‐butyl acrylate (tBA)‐based polymer, which has a glass transition temperature of 60 °C. The AFM tip forms indents in the polymer in the temperature range 25–250 °C. The shape recovery of the indents is studied while the polymer is heated up to 100 °C. The temperature required for complete annealing of the indents depends upon the indentation formation conditions, with higher temperature formation corresponding to higher temperature recovery. SCANNING 29: 000–V000, 2007. © 2007 Wiley Periodicals, Inc.

The content you want is available to Zendy users.

Already have an account? Click here to sign in.
Having issues? You can contact us here
Accelerating Research

Address

John Eccles House
Robert Robinson Avenue,
Oxford Science Park, Oxford
OX4 4GP, United Kingdom