Mass spectrometric studies of cyclopentanol derivatives in the reductive coupling of  α , β ‐unsaturated ketones assisted by samarium diiodide | Zendy

Le Lagadec Ronan | Zendy; Rubio Laura | Zendy; Velasco Luis | Zendy; PérezFlores Javier | Zendy; Miranda Rene | Zendy; Cabrera Armando | Zendy

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Mass spectrometric studies of cyclopentanol derivatives in the reductive coupling of α , β ‐unsaturated ketones assisted by samarium diiodide

Author(s) -

Le Lagadec Ronan,

Rubio Laura,

Velasco Luis,

PérezFlores Javier,

Miranda Rene,

Cabrera Armando

Publication year - 2003

Publication title -

rapid communications in mass spectrometry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.528

H-Index - 136

eISSN - 1097-0231

pISSN - 0951-4198

DOI - 10.1002/rcm.1108

Subject(s) - chemistry , deuterium , samarium diiodide , samarium , molecule , computational chemistry , analytical chemistry (journal) , medicinal chemistry , organic chemistry , atomic physics , physics

The mass spectrometric fragmentations of a series of cyclopentanol derivatives in positive fast‐atom bombardment (FAB + ) mode were investigated. The corresponding pathways proposed were confirmed by MS/MS data obtained using linked scans at constant B/E, high‐resolution accurate mass data, and comparisons with corresponding information for a specifically deuterated molecule. Copyright © 2003 John Wiley & Sons, Ltd.

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