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Quantitative electron microscopy of InN–GaN alloys
Author(s) -
Bartel T.,
Jinschek J. R.,
Freitag B.,
Specht P.,
Kisielowski C.
Publication year - 2006
Publication title -
physica status solidi (a)
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.532
H-Index - 104
eISSN - 1862-6319
pISSN - 1862-6300
DOI - 10.1002/pssa.200563511
Subject(s) - indium , spinodal decomposition , acceleration voltage , materials science , lattice (music) , electron , lattice constant , electron microscope , band gap , condensed matter physics , analytical chemistry (journal) , chemistry , optoelectronics , cathode ray , physics , optics , diffraction , quantum mechanics , organic chemistry , chromatography , acoustics , phase (matter)
Time series of high‐resolution lattice images are examined to probe for possible alterations of the indium distribution in GaN/In x Ga 1– x N/GaN quantum well structures during electron irradiation with energies of 150 kV and 800 kV. By comparison with theory it is reasoned that sample preparation, microscope stability, and chosen acceleration voltages are essential factors that determine the reliability of the results. If considered, it is shown that for relevant time scales of <2 minutes and current densities of 20–40 A/cm 2 no measurable alteration of the initial element distribution occurs. A quantitative method is highlighted for the characterization of existing indium fluctuations that are concentration dependent. Consistency between measurements from lattice images, Z‐contrast images, and local band gap measurements support our conclusion. It is argued that the formation of such indium clusters is driven by strain‐dependent spinodal decomposition. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)