An Efficient and Facile Synthesis of CL‐20 from TADNO Using HNO 3 /N 2 O 5  and Optimization of Reaction Parameters by Taguchi Method | Zendy

Bayat Yadollah | Zendy; Hajighasemali Fatemeh | Zendy

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An Efficient and Facile Synthesis of CL‐20 from TADNO Using HNO 3 /N 2 O 5 and Optimization of Reaction Parameters by Taguchi Method

Author(s) -

Bayat Yadollah,

Hajighasemali Fatemeh

Publication year - 2016

Publication title -

propellants, explosives, pyrotechnics

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.56

H-Index - 65

eISSN - 1521-4087

pISSN - 0721-3115

DOI - 10.1002/prep.201500347

Subject(s) - taguchi methods , propellant , yield (engineering) , reaction conditions , materials science , explosive material , analytical chemistry (journal) , nuclear chemistry , chemistry , organic chemistry , metallurgy , catalysis , composite material

Hexanitrohexaazaisowurtzitane (CL‐20) is an outstanding member of a promising new class of energetic compounds, which is applicable in both propellants and explosives. Herein, CL‐20 was synthesized in an efficient method from tetraacetyldinitrosohexaazaisowurtzitane (TADNO) using N 2 O 5 /HNO 3 . The optimization reaction parameters were performed according to the Taguchi OA method. The yield of reaction at the optimized conditions was 97 % with 98.75 % purity.

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