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Application of Thin Layer Chromatography for Monitoring of FOX‐7 Synthesis
Author(s) -
Błądek Jan,
Pietrzyk Sylwia,
Cudziło Stanisław,
Chyłek Zbigniew
Publication year - 2009
Publication title -
propellants, explosives, pyrotechnics
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.56
H-Index - 65
eISSN - 1521-4087
pISSN - 0721-3115
DOI - 10.1002/prep.200700268
Subject(s) - thin layer chromatography , chromatography , chemistry
Abstract In this paper, results of the research on the application of thin layer chromatography (TLC) for the determination of 1,1‐diamino‐2,2‐dinitroethene (FOX‐7, DADNE) and its precursors produced in the synthetic path starting from 2‐methylpyrimidine‐4,6(1H,5H)‐dione are presented. Analytical parameters of the substances and methodology of their quantitative analysis were determined, and the results obtained were used for monitoring the FOX‐7 synthesis process.