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Heat of Fusion for 1,3,5,5‐ Tetranitrohexahydropyrimidine (DNNC) and its DNNC‐d 6 deuterium labelled analogue
Author(s) -
Shackelford Scott A.,
Goldman Jeffrey F.
Publication year - 1995
Publication title -
propellants, explosives, pyrotechnics
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.56
H-Index - 65
eISSN - 1521-4087
pISSN - 0721-3115
DOI - 10.1002/prep.19950200102
Subject(s) - differential scanning calorimetry , fusion , enthalpy of fusion , deuterium , melting point , confidence interval , calorimetry , analytical chemistry (journal) , chemistry , materials science , thermodynamics , mathematics , physics , chromatography , statistics , nuclear physics , organic chemistry , linguistics , philosophy
The heat of fusion for DNNC (1,3,5,5‐tetranitrohexahydropyrimidine) and its DNNC‐d 6 analogue compound have been determined using differential scanning calorimetry analysis. No significant difference in the DNNC and DNNC‐d 6 heat of fusion values was detected at the 95 and 99 percent student t confidence levels. Melting points were also determined for the subject compounds using this analysis technique. These melting points are compared to literature values obtained by conventional methods.