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Processing effects in production of composite prepreg by hot melt impregnation
Author(s) -
Chmielewski C.,
Jayaraman K.,
Petty C. A.
Publication year - 1993
Publication title -
polymer composites
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.577
H-Index - 82
eISSN - 1548-0569
pISSN - 0272-8397
DOI - 10.1002/pc.750140311
Subject(s) - materials science , composite material , composite number , viscosity , mass fraction
The hot melt impregnation process for producing composite prepreg has been studied. The role of the exit die is highlighted by operating without impregnation bars. Experimental results show that when a fiber two is pulled through a resin bath and then through a wedge shaped die, the total resin mass fraction and the extent of resin impregnation in the two increase with the processing viscosity. The penetration of resin into a fiber bundle is greater when the resin viscosity is higher . This trend is unchanged over a range of two speeds up to the breaking point. A theoretical model is developed to describe the effect of processing conditions and die geometry on the degree of impregnation. Calculations with this model indicate that for a given die geometry, the degree of impregnation increases from 58% to 90% as the ratio of the clearance between the two and the die wall, to the total die gap is decreased from 0.15 to 0.05. Physical arguments elated to the effective viscosity of the prepreg show that the clearance ratio is independent of the two speed, but decreases as the ratio of the effective shear viscosity of the prepareg to the resin viscosity increases. This provides a connection between the experimental results obtained with varying resin viscosity and the computational results obtained with varying clearance values at the die inlet.