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Trends in solid‐state structures were used to identify preferred intramolecular movements in half‐sandwich compounds [CpFe(CO){C(=O)R}PPh 3 ]. Three weak interactions were analyzed: 1) the CH/π donor–acceptor interaction of phenyl rings in the PPh 3  ligand, 2) the Ph PPh3  face‐on Cp stabilization, and 3) the hydrogen bond between the oxygen atom of the acyl group and an  ortho ‐C−H bond of one of the PPh 3  phenyl rings. Clockwise and counter‐clockwise rotations established directed and coupled movements of the PPh 3  ligand, the acyl group, and the phenyl rings within the PPh 3  ligand.

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Trend‐Analysis of Solid‐State Structures: Low‐Energy Conformational ‘Reactions’ Involving Directed and Coupled Movements in Half‐Sandwich Compounds [CpFe(CO){C(=O)R}PPh 3 ]