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The development of a protocol for the reductive functionalization of amides into  N ‐sulfonylformamidines is reported. The one‐pot procedure is based on a mild catalytic reduction of tertiary amides into the corresponding enamines by the use of Mo(CO) 6  (molybdenum hexacarbonyl) and TMDS (1,1,3,3‐tetramethyldisiloxane). The formed enamines were allowed to react with sulfonyl azides to give the target compounds in moderate to good yields.

Mild Reductive Functionalization of Amides into N ‐Sulfonylformamidines